
Updated:
26.06.2007
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Data collection
Two diffractometers
are available for data collection at the PX X06SA beamline.
The High Resolution Diffractometer, and,
for very small sample sizes, the Micro Crystal Diffractometer MD2.
Currently the energy can be changed with the
appropriate IDL command
(sete,e).
Energy - Wavelength
| E / keV |
5 | 6 | 7 | 8 | 9 | 10 | 11 | 12 |
13 | 14 | 15 | 16 | 17 | 18 | 19 | 20 |
| λ / Å |
2.4797 | 2.0664 | 1.7712 | 1.5498 | 1.3776 | 1.2399 | 1.1271 |
1.0332 |
0.9537 | 0.8856 | 0.8266 | 0.7749 | 0.7293 | 0.6888 | 0.6526 |
0.6199 |
Converter
Cooling time scale at the beamlines
The following graphic shows the temperature curve for the cryojet, after being
heated from 100 K to 150 K, and cooled down to 100 K again.
General guidelines for data collection
- Users are ultimately responsible for their data collection strategy and the data they get, barring any obvious flaw
in the hardware.
Therefore, ask for advice but do not follow it blindly.
- Immediately process all your data, even while they are being collected. Thus, you will be able to identify problems
and you might re-collect if necessary.
- Let the beamline staff know about possible problems! If there is a problem with the hard- or software, it will be taken care
of.
If you do not give feedback, improvements might take longer.
- After data collection, please submit an end-of-run report via your
DUO account!
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